蜂蜜真伪鉴别及检测方法研究-农业与食品科学-CSCIED科技核心评价数据库-手机版

蜂蜜真伪鉴别及检测方法研究

Study on the identification and detection methods of honey authenticity

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DOI	10.12208/j.jafs.20230012
刊名	农业与食品科学 Journal of Agriculture and Food Science
年，卷(期)	2023, 3(2)
作者	张波,王楠楠*,袁婧威,
作者单位	承德市食品药品检验检测中心河北承德 ;
摘要	为了建立蜂蜜检测方法以及进行真伪鉴别，以市场及蜂农处购买的共计40个不同产地、不同蜜源的蜂蜜为研究样本，通过近红外光谱法对真实蜂蜜和一定比例的糖浆进行测定，对比二者区别。利用电感耦合等离子质谱仪（ICP-MS）和液相色谱仪对蜂蜜中的26种不同元素和8种酚酸及黄酮的种类及含量建立方法并对其进行方法学验证，应用已建立的方法对所购买的样本测定分析。通过实验结果可知，红外光谱法对于蜂蜜的掺杂检测能够提供一定的支持，不同种类、不同产地的蜂蜜样本中元素含量及酚酸和黄酮的含量有所差异。测定结果可为今后研究及方法制定提供理论依据。
Abstract	In order to establish a honey detection method and identify authenticity, a total of 40 honey samples from different origins and sources purchased by the market and bee farmers were used as research samples. Real honey and a certain proportion of syrup were measured using near-infrared spectroscopy to compare their differences. A method was established using inductively coupled plasma mass spectrometry (ICP-MS) and liquid chromatography to determine the types and contents of 26 different elements, 8 phenolic acids, and flavonoids in honey. The established method was applied to determine and analyze the purchased samples. According to the experimental results, infrared spectroscopy can provide certain support for the doping detection of honey, and the element content, phenolic acid and flavonoid content in honey samples from different types and origins vary. The measurement results can provide a theoretical basis for future research and method development.
关键词	蜂蜜；近红外光谱；电感耦合等离子质谱；液相色谱；矿物质；酚酸和黄酮类化合物
KeyWord	Honey; Near-infrared spectroscopy; Inductively coupled plasma mass spectrometry; Liquid chromatography; Minerals; Phenolic acids; Flavonoids
基金项目
页码	14-20

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[1] Machado De-Melo A A, Almeida-Muradian L B D, Sancho M T, et al. Composition and properties of Apis mellifera honey: A review
[J]. Journal of Apicultural Research, 2018, 57(1): 5-37.

[2] Naila A, Flint S H, Sulaiman A Z, et al. Classical and novel approaches to the analysis of honey and detection of adulterants
[J]. Food Control, 2018, 90: 152-165.

[3] Hossen M S, Ali M Y, Jahurul M H A, et al. Beneficial roles of honey polyphenols against some human degenerative diseases: A review
[J]. Pharmacological Reports, 2017, 69(6): 1194-1205.

[4] Khan S U, Anjum S I, Rahman K, et al. Honey: Single food stuff comprises many drugs
[J]. Saudi Journal of Biological Sciences, 2018, 25(2): 320-325.

[5] Meo S A, Al-Asiri S A, Mahesar A L, et al. Role of honey in modern medicine
[J]. Saudi Journal of Biological Sciences, 2017, 24(5): 975-978.

[6] White J W, Riethof M L, Subers M H, et al.Technical Bulletin, 1962, 1261:1.

[7] Bokobza L. Near Infrared Spectroscopy
[J]. J Near Infrared Spec-trosc, 1998,6:3-17.

[8] Batten GD. An Appreciation of the Contribution of NIR to Agri-culture
[J].J Near Infrared Spectrosc, 1998,6:105-114.

[9] 岳锦萍,徐雨欣,范佳慧,等.蜂蜜的主要成分及其鉴别技术
[J].食品安全质量检测学报,2018,9(19):5138-5145.

[10] 刘芸, 丁涛, 吴斌, 等. 核磁共振技术结合化学计量学方法用于蜂蜜的掺假鉴别
[J]. 分析测试学报, 2016, 35(10): 1248-1254.

[11] 孙丽萍, 穆雪峰, 施海燕, 等. 北京洋槐蜜化学成分及其抗氧化活性
[C]. 全国蜂产品市场信息交流会, 2012: 77−80.

[12] 张敏,黄京平,赵文等.超高效液相色谱-串联质谱法测定蜂蜜中24种酚酸和黄酮类化合物
[J].分析测试学报, 2022, 41(11): 1636-1643.

[13] 孙崇臻,王超,蔡子哲,等.高效液相色谱测定蜂蜜中的脱落酸、黄酮和酚酸
[J].食品科学,2013,34(10):281-285.

引用本文

张波,王楠楠*,袁婧威. 蜂蜜真伪鉴别及检测方法研究 [J]. 农业与食品科学. 2023; 3; (2). 14 - 20.

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